{"id":4077,"date":"2024-08-04T08:21:45","date_gmt":"2024-08-04T08:21:45","guid":{"rendered":"https:\/\/longchangextracts.com\/?p=4077"},"modified":"2024-08-04T08:21:45","modified_gmt":"2024-08-04T08:21:45","slug":"anion-resins","status":"publish","type":"post","link":"https:\/\/longchangextracts.com\/tr\/anyon-recineleri\/","title":{"rendered":"Oleuropeinin Anyonik Re\u00e7ine ile Ayr\u0131\u015ft\u0131r\u0131lmas\u0131 S\u00fcreci ve Performans\u0131 \u00dczerine \u00c7al\u0131\u015fma"},"content":{"rendered":"

Oleuropeinin Anyonik Re\u00e7ine ile Ayr\u0131\u015ft\u0131r\u0131lmas\u0131 S\u00fcreci ve Performans\u0131 \u00dczerine \u00c7al\u0131\u015fma
\nOlea europaea L., Oleaceae familyas\u0131na ve Oleaceae cinsine ait yaprak d\u00f6kmeyen bir a\u011fa\u00e7t\u0131r. \u00c7in ve Akdeniz \u00fclkelerinde yayg\u0131n olarak ekilir ve bu \u00fclke ve b\u00f6lgelerde ba\u015fl\u0131ca tar\u0131msal nakit \u00fcr\u00fcnlerinden biridir. \u015eu anda, zeytin kaynaklar\u0131n\u0131n geli\u015ftirilmesi ve kullan\u0131m\u0131 esas olarak meyvelerin kullan\u0131m\u0131na odaklan\u0131rken, zeytin yapraklar\u0131 plantasyonlarda at\u0131k olarak terk edilmekte ve b\u00fcy\u00fck kaynak israf\u0131na neden olmaktad\u0131r. Modern ara\u015ft\u0131rmalar zeytin yapraklar\u0131n\u0131n bol miktarda iridoid glikozitler, fenoller, pentasiklik triterpenoidler ve flavonoidler i\u00e7erdi\u011fini ortaya koymu\u015ftur. Bunlar aras\u0131nda, oleuropein (OL) antioksidan, antiviral, bakterisidal ve anti-inflamatuar, hipoglisemik, antihipertansif, anti-kanser ve di\u011fer etkilere sahip olan ve g\u0131da, ila\u00e7, kozmetik ve di\u011fer alanlarda yayg\u0131n olarak kullan\u0131lan en aktif maddedir. OL, su, etanol ve metanol gibi \u00e7\u00f6z\u00fcc\u00fclerde kolayca \u00e7\u00f6z\u00fcnebilen iridoid glikozitler s\u0131n\u0131f\u0131na aittir. Asit, alkali, y\u00fcksek s\u0131cakl\u0131k ve \u0131\u015f\u0131k gibi ko\u015fullar alt\u0131nda kolayca hidroksitirosole ayr\u0131\u015fabilirler.
\n\u015eu anda, OL'yi ay\u0131rmak i\u00e7in kullan\u0131lan ana y\u00f6ntemler aras\u0131nda makrog\u00f6zenekli re\u00e7ine adsorpsiyonu, y\u00fcksek h\u0131zl\u0131 ters ak\u0131m ekstraksiyonu ve s\u00fcperkritik ekstraksiyon bulunmaktad\u0131r. Bunlar aras\u0131nda, y\u00fcksek h\u0131zl\u0131 ters ak\u0131ml\u0131 ekstraksiyon ve s\u00fcperkritik ekstraksiyon daha iyi ay\u0131rma etkilerine sahiptir ve y\u00fcksek safl\u0131kta OL elde edebilir. Bununla birlikte, bu iki y\u00f6ntem y\u00fcksek ekipman ve personel operasyonu gerektirir ve b\u00fcy\u00fck \u00f6l\u00e7ekli end\u00fcstriyel \u00fcretim i\u00e7in uygun de\u011fildir. Makrog\u00f6zenekli re\u00e7ine g\u00f6zenekli bir yap\u0131ya ve m\u00fckemmel adsorpsiyon performans\u0131na sahiptir ve bitki aktif bile\u015fenlerinin zenginle\u015ftirilmesi, ayr\u0131lmas\u0131 ve safla\u015ft\u0131r\u0131lmas\u0131 i\u00e7in yayg\u0131n olarak kullan\u0131lmaktad\u0131r. OL'nin makro g\u00f6zenekli re\u00e7ine ile zenginle\u015ftirilmesi ve ayr\u0131lmas\u0131n\u0131n ana mekanizmas\u0131, ikisinin belirli ko\u015fullar alt\u0131nda hidrojen ba\u011f\u0131 ve van der Waals kuvvetleri yoluyla tersine \u00e7evrilebilir etkile\u015fimlere girebilmesi ve b\u00f6ylece se\u00e7ici olarak zenginle\u015ftirilmesi ve ekstraksiyon \u00e7\u00f6zeltisinden ayr\u0131lmas\u0131d\u0131r. Son y\u0131llarda, bir\u00e7ok bilim insan\u0131 polar olmayan ve zay\u0131f polar re\u00e7ineler kullanarak zeytin yapra\u011f\u0131 ekstraktlar\u0131nda OL'nin zenginle\u015ftirilmesi ve ayr\u0131lmas\u0131 \u00fczerine odaklanm\u0131\u015ft\u0131r. Tian ve arkada\u015flar\u0131 OL'yi zenginle\u015ftirmek ve ay\u0131rmak i\u00e7in makro g\u00f6zenekli re\u00e7ine D101 kullanm\u0131\u015f ve etil asetat ekstraksiyonu yoluyla 63.43% safl\u0131\u011f\u0131nda OL \u00fcr\u00fcn\u00fc elde etmi\u015ftir. Wang ve arkada\u015flar\u0131 OL'yi zenginle\u015ftirmek ve ay\u0131rmak i\u00e7in AB-8 re\u00e7inesini kullanm\u0131\u015f ve safl\u0131k 9.16%'den 20.38%'ye y\u00fckselmi\u015ftir. \u015eahin ve arkada\u015flar\u0131, XAD 7HP re\u00e7inesinin OL'yi adsorbe etme mekanizmas\u0131n\u0131n ikinci dereceden kineti\u011fe uygun oldu\u011funu bulmu\u015flard\u0131r. Liu ve arkada\u015flar\u0131, OL'nin makro g\u00f6zenekli adsorpsiyon re\u00e7inesi BMKX-4 taraf\u0131ndan zenginle\u015ftirilme mekanizmas\u0131n\u0131n ikinci dereceden kinetik ve Freundlich modeline uygun oldu\u011funu ve OL'nin safl\u0131\u011f\u0131n\u0131 47.59%'ye y\u00fckseltti\u011fini bulmu\u015flard\u0131r. Teorik olarak, OL polifenolik bile\u015fiklere aittir ve anyonik re\u00e7inenin adsorpsiyon mekanizmas\u0131 zenginle\u015ftirilmesini ve ayr\u0131lmas\u0131n\u0131 sa\u011flayabilir. Bununla birlikte, OL'nin anyon re\u00e7inesi ile ayr\u0131\u015ft\u0131r\u0131lmas\u0131 ara\u015ft\u0131rmas\u0131 hakk\u0131nda herhangi bir rapor bulunmamaktad\u0131r. Bu nedenle, OL'nin statik ve dinamik adsorpsiyon ve desorpsiyon \u00f6zelliklerini incelemek i\u00e7in anyon re\u00e7inesi (LX-68M) kulland\u0131k ve OL ve benzeri do\u011fal \u00fcr\u00fcnlerin anyon re\u00e7inesi ile zenginle\u015ftirilmesi, ayr\u0131lmas\u0131, safla\u015ft\u0131r\u0131lmas\u0131 i\u00e7in teorik referans sa\u011flamak amac\u0131yla s\u0131z\u0131nt\u0131 e\u011frisini, el\u00fcsyon e\u011frisini ve OL'nin anyon re\u00e7inesi rejenerasyonunun stabilitesini daha fazla ara\u015ft\u0131rd\u0131k.<\/p>\n

\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"<\/p>\n

\u0130zotermal adsorpsiyon deney sonu\u00e7lar\u0131, Freundlich izotermal adsorpsiyon modelinin deneysel s\u0131cakl\u0131kta LX-68M re\u00e7inesinin OL'yi adsorbe etme s\u00fcrecini iyi bir \u015fekilde tan\u0131mlayabildi\u011fini ve R2=0.9642 korelasyon katsay\u0131s\u0131 ile adsorpsiyonun uygun oldu\u011funu g\u00f6stermektedir. OL'nin LX-68M re\u00e7inesi taraf\u0131ndan adsorpsiyonu, R2=0,9934 ile s\u00f6zde ikinci derece kineti\u011fe daha uygundur; bu da OL'nin LX-68M re\u00e7inesi taraf\u0131ndan adsorpsiyonunun fiziksel adsorpsiyon ve kimyasal adsorpsiyon yoluyla e\u015fzamanl\u0131 olarak ger\u00e7ekle\u015fti\u011fini ve kimyasal adsorpsiyonun ana mekanizma oldu\u011funu g\u00f6sterir. Mekanizma, re\u00e7inenin fonksiyonel gruplar\u0131 ile OL aras\u0131nda kimyasal ba\u011flar\u0131n olu\u015fmas\u0131 olabilir. Statik ve dinamik adsorpsiyon ve desorpsiyon deneyleriyle elde edilen optimum ay\u0131rma ko\u015fullar\u0131 \u015funlard\u0131r: 0.25g\/mL ekstraksiyon konsantrasyonu, 45% etanol eluenti, 2.0BV\/sa y\u00fckleme h\u0131z\u0131, 6. 0BV y\u00fckleme hacmi, 6. 0BV desorpsiyon h\u0131z\u0131.0BV, desorpsiyon oran\u0131 2.0BV\/h ve desorpsiyon hacmi 10.0BV; Bu s\u0131rada adsorpsiyon oran\u0131 ve desorpsiyon oran\u0131 s\u0131ras\u0131yla 86.86% ve 87.08% ve elde edilen OL safl\u0131\u011f\u0131 52.33% idi. 4 d\u00f6ng\u00fc re\u00e7ine adsorpsiyon desorpsiyonundan sonra, adsorpsiyon verimlili\u011fi 54.9% olmu\u015ftur. Rejenerasyondan sonra, adsorpsiyon oran\u0131 ilk adsorpsiyon oran\u0131n\u0131n 93.1%'sine ula\u015fm\u0131\u015ft\u0131r, bu da re\u00e7inenin rejenerasyondan sonra hala iyi adsorpsiyon performans\u0131na sahip oldu\u011funu g\u00f6stermektedir. Yukar\u0131daki sonu\u00e7lar, LX-68M re\u00e7inesinin OL i\u00e7in iyi bir zenginle\u015ftirme, ay\u0131rma ve safla\u015ft\u0131rma verimlili\u011fine sahip oldu\u011funu ve mevcut i\u015flemlerle kar\u015f\u0131la\u015ft\u0131r\u0131ld\u0131\u011f\u0131nda, bu i\u015flemin oda s\u0131cakl\u0131\u011f\u0131nda ve bas\u0131n\u00e7ta \u00e7al\u0131\u015ft\u0131\u011f\u0131n\u0131, g\u00fcvenli ve basit oldu\u011funu ve ye\u015fil ve toksik olmayan \u00e7\u00f6z\u00fcc\u00fcler kulland\u0131\u011f\u0131n\u0131 g\u00f6stermektedir. OL ve benzeri do\u011fal \u00fcr\u00fcnlerin end\u00fcstriyel olarak ayr\u0131\u015ft\u0131r\u0131lmas\u0131 ve safla\u015ft\u0131r\u0131lmas\u0131nda anyonik re\u00e7inenin uygulanmas\u0131 i\u00e7in teorik ara\u015ft\u0131rma temeli ve teknik destek sa\u011flayabilir. Bu \u00e7al\u0131\u015fma LX-68M re\u00e7inesinin OL \u00fczerindeki adsorpsiyon s\u00fcrecini incelemi\u015f olsa da, safs\u0131zl\u0131klar ve OL aras\u0131ndaki rekabet\u00e7i adsorpsiyon davran\u0131\u015f\u0131n\u0131n da ay\u0131rma verimlili\u011fi \u00fczerinde belirli bir etkisi olabilir. Bu nedenle, ilgili adsorpsiyon mekanizmas\u0131n\u0131 belirlemek ve LX-68M re\u00e7inesinin daha fazla geli\u015ftirilmesi ve kullan\u0131lmas\u0131 i\u00e7in teorik temel sa\u011flamak i\u00e7in daha fazla ara\u015ft\u0131rmaya ihtiya\u00e7 vard\u0131r.<\/p>","protected":false},"excerpt":{"rendered":"

Study on the Process and Performance of Separation of Oleuropein by Anionic Resin Olea europaea L. is an evergreen tree belonging to the Oleaceae family and the Oleaceae genus. It is widely planted in China and Mediterranean countries and is one of the main agricultural cash crops in these countries and regions. At present, the […]<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[20],"tags":[],"yoast_head":"\nStudy on the Process and Performance of Separation of Oleuropein by Anionic Resin - China Chemical Manufacturer<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/longchangextracts.com\/tr\/anyon-recineleri\/\" \/>\n<meta property=\"og:locale\" content=\"tr_TR\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Study on the Process and Performance of Separation of Oleuropein by Anionic Resin - China Chemical Manufacturer\" \/>\n<meta property=\"og:description\" content=\"Study on the Process and Performance of Separation of Oleuropein by Anionic Resin Olea europaea L. is an evergreen tree belonging to the Oleaceae family and the Oleaceae genus. 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