{"id":6893,"date":"2024-08-06T15:05:27","date_gmt":"2024-08-06T15:05:27","guid":{"rendered":"https:\/\/longchangextracts.com\/?p=6893"},"modified":"2024-08-06T15:05:27","modified_gmt":"2024-08-06T15:05:27","slug":"four-components-in-turmeric-standard-decoction","status":"publish","type":"post","link":"https:\/\/longchangextracts.com\/hu\/four-components-in-turmeric-standard-decoction\/","title":{"rendered":"UPLC-ujjlenyomat l\u00e9trehoz\u00e1sa \u00e9s n\u00e9gy komponens mennyis\u00e9gi elemz\u00e9se a kurkuma standard f\u0151zet\u00e9ben"},"content":{"rendered":"

UPLC-ujjlenyomat l\u00e9trehoz\u00e1sa \u00e9s n\u00e9gy komponens mennyis\u00e9gi elemz\u00e9se a kurkuma standard f\u0151zet\u00e9ben
\nA t\u00f6bb ezer \u00e9ves gy\u00f3gy\u00e1szati gyakorlat ut\u00e1n a f\u0151zetek m\u00e9g mindig a hagyom\u00e1nyos k\u00ednai orvosl\u00e1s f\u0151 adagol\u00e1si form\u00e1ja a klinikai alkalmaz\u00e1sban. A t\u00e1rsadalom fejl\u0151d\u00e9s\u00e9vel \u00e9s a technol\u00f3gia fejl\u0151d\u00e9s\u00e9vel a f\u0151zetek \u00faj \"jelent\u00e9startalmakat\" kaptak, \u00e9s a hagyom\u00e1nyos k\u00ednai orvosl\u00e1s \"standard f\u0151zete\" is kialakult. A k\u00ednai orvosl\u00e1s standard f\u0151zet egy standard anyag, amelyet a hagyom\u00e1nyos k\u00ednai orvosl\u00e1s f\u0151z\u00e9si m\u00f3dszer\u00e9re hivatkozva \u00e9s egy standardiz\u00e1lt f\u0151z\u00e9si m\u00f3dot alkalmazva \u00e1ll\u00edtanak el\u0151. Ez szabv\u00e1nyos\u00edthatja a k\u00ednai gy\u00f3gy\u00e1szat klinikai alkalmaz\u00e1s\u00e1t, szabv\u00e1nyos\u00edthatja az \u00faj k\u00ednai gy\u00f3gy\u00e1szati f\u0151zetdarabok, mint p\u00e9ld\u00e1ul a k\u00ednai gy\u00f3gy\u00e1szati formula granulumok haszn\u00e1lat\u00e1t a klinikai gyakorlatban, \u00e9s hivatkoz\u00e1si alapot biztos\u00edthat a k\u00ednai gy\u00f3gy\u00e1szati formula granulumok, a klasszikus formula k\u00e9sz\u00edtm\u00e9nyek \u00e9s m\u00e1s term\u00e9kek kutat\u00e1s\u00e1hoz \u00e9s fejleszt\u00e9s\u00e9hez.
\nA kurkuma a Curcuma longa L., a gy\u00f6mb\u00e9rf\u00e9l\u00e9k csal\u00e1dj\u00e1ba tartoz\u00f3 Curcuma longa L. sz\u00e1r\u00edtott riz\u00f3m\u00e1ja. V\u00e9rt\u00f6r\u0151, qi-kering\u00e9st el\u0151seg\u00edt\u0151 \u00e9s f\u00e1jdalomcsillap\u00edt\u00f3 hat\u00e1s\u00fa. A klinikai gyakorlatban gyakran haszn\u00e1lt hagyom\u00e1nyos k\u00ednai gy\u00f3gy\u00e1szatban. A kurkuma f\u0151 k\u00e9miai \u00f6sszetev\u0151i fenolok \u00e9s terpenoidok. Ezenk\u00edv\u00fcl kis mennyis\u00e9gben tartalmaz alkaloidokat, flavonoidokat, szterolokat is, amelyek antibakteri\u00e1lis, gyullad\u00e1scs\u00f6kkent\u0151, antioxid\u00e1ns, daganatellenes, cukorbetegs\u00e9g elleni, m\u00e1jv\u00e9d\u0151, v\u00e9rzs\u00edrv\u00e9d\u0151 \u00e9s egy\u00e9b hat\u00e1sokkal rendelkeznek. Jelenleg a kurkuma els\u0151sorban Szecsu\u00e1nban, J\u00fcnnanban, Shaanxiban \u00e9s m\u00e1s r\u00e9gi\u00f3kban terjed. Sichuan \u00e9s Yunnan a kurkuma hiteles \u00e9s f\u0151 term\u0151ter\u00fcletei, \u00e9s a piaci k\u00edn\u00e1lat f\u0151k\u00e9nt termesztett. Kev\u00e9s vadon term\u0151 forr\u00e1s van, ami megnehez\u00edti a sk\u00e1la kialak\u00edt\u00e1s\u00e1t. Jelenleg a kurkuma min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9se els\u0151sorban a kurkumin komponensek \u00e9s az ill\u00f3olajok elemz\u00e9s\u00e9re \u00e9s meghat\u00e1roz\u00e1s\u00e1ra \u00f6sszpontos\u00edt, m\u00e1s t\u00edpus\u00fa komponensekkel kapcsolatban kevesebb kutat\u00e1s folyik.
\nA modern analitikai technol\u00f3gia fejl\u0151d\u00e9s\u00e9vel jelent\u0151s el\u0151rel\u00e9p\u00e9s t\u00f6rt\u00e9nt a hagyom\u00e1nyos k\u00ednai orvosl\u00e1s min\u0151s\u00e9gellen\u0151rz\u00e9s\u00e9ben. Az olyan min\u0151s\u00e9gellen\u0151rz\u00e9si m\u00f3dok alkalmaz\u00e1sa, mint az ujjlenyomat\/jellemz\u0151 spektrum, az egy m\u00e9r\u00e9s \u00e9s t\u00f6bb \u00e9rt\u00e9kel\u00e9s, a t\u00f6bbkomponens\u0171 mennyis\u00e9gi meghat\u00e1roz\u00e1s \u00e9s a t\u00f6bbkomponens\u0171 v\u00e9konyr\u00e9teg-azonos\u00edt\u00e1s egyre vil\u00e1gosabb\u00e1 tette a hagyom\u00e1nyos k\u00ednai gy\u00f3gy\u00e1szat \"\u00e1tfog\u00f3 min\u0151s\u00e9gellen\u0151rz\u00e9s\u00e9nek\" fogalm\u00e1t. Ez a tanulm\u00e1ny a kurkuma standard f\u0151zet UPLC-ujjlenyomat\u00e1t kemometriai elemz\u00e9ssel kombin\u00e1lva hozta l\u00e9tre a differenci\u00e1lis min\u0151s\u00e9gi markerek azonos\u00edt\u00e1s\u00e1ra, \u00e9s t\u00f6bbkomponens\u0171 mennyis\u00e9gi elemz\u00e9ssel kombin\u00e1lva referencia\u00e9rt\u00e9ket szolg\u00e1ltatott a kurkuma standard f\u0151zet \u00e9s a kapcsol\u00f3d\u00f3 k\u00e9sz\u00edtm\u00e9nyek azonos\u00edt\u00e1s\u00e1hoz \u00e9s min\u0151s\u00e9gellen\u0151rz\u00e9s\u00e9hez.<\/p>\n

\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"
\nA m\u00e9r\u00e9si mutat\u00f3k kiv\u00e1laszt\u00e1sa. A kurkumin \u00e9s az ill\u00f3olaj a kurkuma egyik f\u0151 akt\u00edv \u00f6sszetev\u0151je, de v\u00edzben val\u00f3 oldhat\u00f3s\u00e1guk viszonylag alacsony. A szabv\u00e1nyos f\u0151zetek old\u00f3szerk\u00e9nt vizet haszn\u00e1lnak, \u00e9s a v\u00edzben old\u00f3d\u00f3 komponenseknek fontos anyagi alapot kell k\u00e9pezni\u00fck a f\u0151zetek hat\u00e9konys\u00e1g\u00e1nak meghat\u00e1roz\u00e1s\u00e1hoz. Ez\u00e9rt a szabv\u00e1nyos f\u0151zetek min\u0151s\u00e9gi szabv\u00e1nyainak tanulm\u00e1nyoz\u00e1sa sor\u00e1n a kurkuma komponensek m\u00e9r\u00e9se mellett a ferulasav meghat\u00e1roz\u00e1s\u00e1t is hozz\u00e1adt\u00e1k. A kurkumin komponensekkel \u00f6sszehasonl\u00edtva a ferulasav viszonylag j\u00f3 v\u00edzold\u00e9konys\u00e1ggal rendelkezik, \u00e9s a kurkumin komponensek szint\u00e9zis\u00e9nek el\u0151fut\u00e1ra. Ugyanakkor a standard f\u0151zetek f\u0151z\u00e9si folyamata sor\u00e1n a kurkumin komponensek ferulasavv\u00e1 is \u00e1talakulhatnak. A modern farmakol\u00f3giai kutat\u00e1sok meger\u0151s\u00edtett\u00e9k, hogy a ferulasav antibakteri\u00e1lis, antivir\u00e1lis, antioxid\u00e1ns, antitrombotikus, lipidcs\u00f6kkent\u0151, a sz\u00edvizom iszk\u00e9mi\u00e1t \u00e9s az oxig\u00e9nfogyaszt\u00e1st cs\u00f6kkent\u0151 hat\u00e1ssal rendelkezik, \u00e9s gy\u00f3gy\u00e1szati \u00e9rt\u00e9ke egyre fontosabb\u00e1 v\u00e1lik. Figyelmet ford\u00edtanak a ferulasav mennyis\u00e9g\u00e9re a standard f\u0151zetben, T\u00fckr\u00f6zi a kurkuma k\u00e9miai \u00f6sszet\u00e9tel\u00e9nek v\u00e1ltoz\u00e1sait a standard f\u0151z\u00e9si folyamat sor\u00e1n. A modern hagyom\u00e1nyos k\u00ednai gy\u00f3gyszerk\u00e9sz\u00edtm\u00e9nyek, p\u00e9ld\u00e1ul a \"standard f\u0151zeteken\" alapul\u00f3 granul\u00e1tumok gy\u00e1rt\u00e1si folyamatainak optimaliz\u00e1l\u00e1sa er\u0151s ir\u00e1nymutat\u00f3 jelent\u0151s\u00e9ggel b\u00edr.<\/p>\n

Analitikai m\u00f3dszerek meg\u00e1llap\u00edt\u00e1sa. A kurkuma standard f\u0151zet\u00e9ben l\u00e9v\u0151 k\u00e9miai \u00f6sszetev\u0151k polarit\u00e1sa nagym\u00e9rt\u00e9kben v\u00e1ltozik, bele\u00e9rtve a nagy lipidold\u00e9konys\u00e1g\u00fa akt\u00edv \u00f6sszetev\u0151ket, mint p\u00e9ld\u00e1ul a kurkumin, \u00e9s a v\u00edzben old\u00f3d\u00f3 \u00f6sszetev\u0151ket, mint p\u00e9ld\u00e1ul a ferulasav. Ez\u00e9rt az ujjlenyomat-spektrum meg\u00e1llap\u00edt\u00e1s\u00e1hoz a fenti komponensek maxim\u00e1lis extrakci\u00f3j\u00e1ra van sz\u00fcks\u00e9g, ugyanakkor figyelembe kell venni a k\u00fcl\u00f6nb\u00f6z\u0151 polarit\u00e1s\u00fa k\u00e9miai komponensek j\u00f3 kromatogr\u00e1fi\u00e1s elv\u00e1laszt\u00e1s\u00e1t, \u00e9s az ujjlenyomat-spektrum felt\u00e9teleivel \u00f6sszhangban l\u00e9v\u0151 t\u00f6bbkomponens\u0171 mennyis\u00e9gi m\u00f3dszert kell l\u00e9trehozni. Ez\u00e9rt a mobilf\u00e1zis-rendszer, a detekt\u00e1l\u00e1si hull\u00e1mhossz \u00e9s a vizsg\u00e1lati oldat elk\u00e9sz\u00edt\u00e9si m\u00f3dj\u00e1nak szisztematikus vizsg\u00e1lat\u00e1t v\u00e9gezt\u00fck el, hogy meghat\u00e1rozzuk a vizsg\u00e1lati oldat optim\u00e1lis kromatogr\u00e1fi\u00e1s felt\u00e9teleit \u00e9s elk\u00e9sz\u00edt\u00e9si m\u00f3dj\u00e1t.
\nAz ujjlenyomat-spektrumok \u00e9s a tartalom meghat\u00e1roz\u00e1si eredm\u00e9nyek \u00e9rt\u00e9kel\u00e9se. A 16 t\u00e9tel kurkuma standard f\u0151zet \u00e9s a kontroll ujjlenyomat-spektrumok k\u00f6z\u00f6tti hasonl\u00f3s\u00e1g 0,95 felett van, ami azt jelzi, hogy az ujjlenyomat-spektrumok \u00e1ltal\u00e1nos hasonl\u00f3s\u00e1ga magas, \u00e9s felhaszn\u00e1lhat\u00f3 a kurkuma standard f\u0151zet azonos\u00edt\u00e1s\u00e1ra \u00e9s min\u0151s\u00e9gellen\u0151rz\u00e9s\u00e9re. A hasonl\u00f3s\u00e1gi sz\u00e1m\u00edt\u00e1s t\u00fckr\u00f6zheti az ujjlenyomat-cs\u00facsok stabil \u00f6sszet\u00e9tel\u00e9t \u00e9s jellemz\u0151 ar\u00e1nyait, de nem k\u00e9pes teljes m\u00e9rt\u00e9kben le\u00edrni \u00e9s megk\u00fcl\u00f6nb\u00f6ztetni az ujjlenyomat-spektrumban tal\u00e1lhat\u00f3 \u00f6sszetett \u00f6sszetev\u0151k eloszl\u00e1si mint\u00e1zat\u00e1t \u00e9s k\u00f6lcs\u00f6nhat\u00e1si kapcsolatait. Ez\u00e9rt a kemometria mintafelismer\u00e9si m\u00f3dszereit haszn\u00e1lt\u00e1k az ujjlenyomat spektrum\u00e1nak vizsg\u00e1lat\u00e1ra. Az eredm\u00e9nyek azt mutatt\u00e1k, hogy a kurkuma standard f\u0151zetmint\u00e1k 16 t\u00e9tele bizonyos termel\u00e9kenys\u00e9ggel rendelkezett, 10 k\u00f6z\u00f6s cs\u00facster\u00fclettel mint v\u00e1ltoz\u00f3kkal, a HCA \u00e9s a PCA egyar\u00e1nt k\u00e9t kateg\u00f3ri\u00e1ba sorolta a 16 t\u00e9telt, a Sichuan termel\u00e9si ter\u00fcletr\u0151l sz\u00e1rmaz\u00f3 mint\u00e1kat az egyik kateg\u00f3ri\u00e1ba, a Yunnan termel\u00e9si ter\u00fcletr\u0151l sz\u00e1rmaz\u00f3 mint\u00e1kat pedig a m\u00e1sik kateg\u00f3ri\u00e1ba sorolta. \u00d6sszesen 6 differenci\u00e1lis biomarkert tal\u00e1ltak, nevezetesen cs\u00facsot, cs\u00facsot (ferulasav), 8. cs\u00facsot (bisz(demetoxikurkum\u00e1n)), 9. cs\u00facsot (demetoxikurkum\u00e1n), 2. cs\u00facsot (vanillin) \u00e9s 1. cs\u00facsot (p-hidroxi-benzaldehid). Az 5. cs\u00facsot nagyfelbont\u00e1s\u00fa t\u00f6megspektrometri\u00e1val azonos\u00edtott\u00e1k, \u00e9s felt\u00e9telezhet\u0151en 1-(4-hidroxi-3,5-dimetoxifenil)-7-(4-hidroxi-3-metoxifenil)-1,4,6-heptadi\u00e9n-3-on lehet. Jelenleg hi\u00e1nyoznak a referenciastandardok, ez\u00e9rt tov\u00e1bbi kutat\u00e1sokra \u00e9s meger\u0151s\u00edt\u00e9sre van sz\u00fcks\u00e9g. A ferulasav, a demetoxikurkumin, a demetoxikurkumin \u00e9s a kurkumin tartalm\u00e1nak m\u00e9r\u00e9s\u00e9vel az eredm\u00e9nyek azt mutatt\u00e1k, hogy a kurkumin, a demetoxikurkumin, a kett\u0151s demetoxikurkumin \u00e9s a ferulasav standard f\u0151zete, amelyet a yunnani Daliban (Dali) tal\u00e1lhat\u00f3 kurkuma nyersanyagokb\u00f3l k\u00e9sz\u00edtettek, magasabb volt, mint a szecsu\u00e1ni Yibinb\u0151l \u00e9s Leshanb\u00f3l sz\u00e1rmaz\u00f3 mint\u00e1k\u00e9. Ez egy\u00fattal referenciak\u00e9nt szolg\u00e1l a v\u00e1llalati termel\u00e9shez sz\u00fcks\u00e9ges nyersanyagok kiv\u00e1laszt\u00e1s\u00e1hoz.
\nJelenleg sz\u00e1mos tanulm\u00e1ny foglalkozik a kurkuma ujjlenyomat-spektrum\u00e1val \u00e9s beltartalm\u00e1nak meghat\u00e1roz\u00e1s\u00e1val, de ezek els\u0151sorban az ill\u00f3olajok \u00e9s a kurkumin komponensek jellemz\u00e9s\u00e9re \u00e9s meghat\u00e1roz\u00e1s\u00e1ra \u00f6sszpontos\u00edtanak, \u00e9s nincs elegend\u0151 kutat\u00e1s a viszonylag nagy v\u00edzold\u00e9konys\u00e1g\u00fa komponensekkel kapcsolatban. Ez a tanulm\u00e1ny meg\u00e1llap\u00edtja a kurkuma standard f\u0151zet UPLC ujjlenyomat spektrum\u00e1t, \u00e9s egyidej\u0171leg meghat\u00e1rozza a n\u00e9gy hat\u00e9kony \u00f6sszetev\u0151t, fontos referenci\u00e1kat biztos\u00edtva a kurkuma gy\u00f3gy\u00e1szati anyagok min\u0151s\u00e9gi szabv\u00e1nyainak jav\u00edt\u00e1s\u00e1hoz, valamint a kurkuma hagyom\u00e1nyos k\u00ednai gy\u00f3gyszerk\u00e9sz\u00edtm\u00e9ny granul\u00e1tumokra \u00e9s klasszikus gy\u00f3gyszerk\u00e9sz\u00edtm\u00e9nyekre vonatkoz\u00f3 term\u00e9kmin\u0151s\u00e9gi szabv\u00e1nyok meg\u00e1llap\u00edt\u00e1s\u00e1hoz. Ez a m\u00f3dszer k\u00f6nnyen kezelhet\u0151, stabil \u00e9s megb\u00edzhat\u00f3, j\u00f3 ism\u00e9telhet\u0151s\u00e9ggel.<\/p>","protected":false},"excerpt":{"rendered":"

Establishment of UPLC fingerprint and quantitative analysis of four components in turmeric standard decoction After thousands of years of medication practice, decoctions are still the main dosage form for clinical use of traditional Chinese medicine. With the development of society and the advancement of technology, decoctions have been given new “connotations”, and the “standard decoctions” […]<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[20],"tags":[],"yoast_head":"\nEstablishment of UPLC fingerprint and quantitative analysis of four components in turmeric standard decoction - China Chemical Manufacturer<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/longchangextracts.com\/hu\/four-components-in-turmeric-standard-decoction\/\" \/>\n<meta property=\"og:locale\" content=\"hu_HU\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Establishment of UPLC fingerprint and quantitative analysis of four components in turmeric standard decoction - China Chemical Manufacturer\" \/>\n<meta property=\"og:description\" content=\"Establishment of UPLC fingerprint and quantitative analysis of four components in turmeric standard decoction After thousands of years of medication practice, decoctions are still the main dosage form for clinical use of traditional Chinese medicine. 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