{"id":5786,"date":"2024-08-04T21:11:05","date_gmt":"2024-08-04T21:11:05","guid":{"rendered":"https:\/\/longchangextracts.com\/?p=5786"},"modified":"2024-08-04T21:11:05","modified_gmt":"2024-08-04T21:11:05","slug":"verbena","status":"publish","type":"post","link":"https:\/\/longchangextracts.com\/hu\/verbena\/","title":{"rendered":"A Verbena min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9s\u00e9nek \u00e9s a standard dekokci\u00f3s adagol\u00e1s \u00e1tviteli t\u00f6rv\u00e9ny\u00e9nek kutat\u00e1sa az UPLC Feature Map \u00e9s az egy teszt t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si m\u00f3dszer alapj\u00e1n"},"content":{"rendered":"

A Verbena min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9s\u00e9nek \u00e9s a standard dekokci\u00f3s adagol\u00e1s \u00e1tviteli t\u00f6rv\u00e9ny\u00e9nek kutat\u00e1sa az UPLC Feature Map \u00e9s az egy teszt t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si m\u00f3dszer alapj\u00e1n
\nA Verbena officinalis L., a Verbenaceae csal\u00e1dba tartoz\u00f3 Verbena officinalis L. n\u00f6v\u00e9ny sz\u00e1raz f\u00f6ld feletti r\u00e9sze, el\u0151sz\u00f6r a \"H\u00edres orvosok katal\u00f3gus\u00e1ban\" ker\u00fclt feljegyz\u00e9sre, \u00e9s alacsonyabb oszt\u00e1lyba sorolt\u00e1k. A verb\u00e9na k\u00e9miai \u00f6sszetev\u0151i f\u0151k\u00e9nt iridoid glikozidok, flavonoidok, szterolok, triterp\u00e9nek, polifenolok, ill\u00f3olajok, tanninok, b\u00e9ta-karotin, k\u00e1v\u00e9sav, cukrok stb. A f\u0151 hat\u00f3anyagok az iridoid glikozidok. H\u0171v\u00f6s jelleg\u0171, keserny\u00e9s \u00edz\u0171, a m\u00e1j \u00e9s a l\u00e9p meridi\u00e1nokhoz tartozik. A v\u00e9rkering\u00e9st el\u0151seg\u00edt\u0151, a v\u00e9r pang\u00e1s\u00e1t eloszlat\u00f3, m\u00e9regtelen\u00edt\u0151, a vizelethajt\u00e1st el\u0151seg\u00edt\u0151, a s\u00e1rgas\u00e1got cs\u00f6kkent\u0151 \u00e9s a mal\u00e1ri\u00e1t elfog\u00f3 hat\u00e1sa van. Klinikailag olyan t\u00fcnetek felhalmoz\u00f3d\u00e1s\u00e1ra haszn\u00e1lj\u00e1k, mint a menstru\u00e1ci\u00f3s zavar, amenorrea, torokgyullad\u00e1s, t\u00e1lyog, \u00f6d\u00e9ma, s\u00e1rgas\u00e1g \u00e9s mal\u00e1ria. A verb\u00e9na er\u0151forr\u00e1sai b\u0151s\u00e9gesek, amelyek k\u00f6z\u00fcl az iridoid glikozidok k\u00fcl\u00f6nb\u00f6z\u0151 hat\u00e1sokkal rendelkeznek, mint p\u00e9ld\u00e1ul antioxid\u00e1ns, hepatoprotekt\u00edv, neuroprotekt\u00edv, sz\u00edv- \u00e9s agyi iszk\u00e9mia elleni v\u00e9d\u0151, gyullad\u00e1scs\u00f6kkent\u0151 stb. A k\u00ednai n\u00f6v\u00e9nyi f\u0151zetek (standard f\u0151zetek) a klinikai gyakorlatban leggyakrabban haszn\u00e1lt hagyom\u00e1nyos k\u00ednai gy\u00f3gyszerk\u00e9sz\u00edtm\u00e9nyek, \u00e9s egyben a k\u00ednai orvosl\u00e1s t\u00f6rt\u00e9net\u00e9ben a legr\u00e9gebben \u00e9s legsz\u00e9lesebb k\u00f6rben haszn\u00e1lt k\u00e9sz\u00edtm\u00e9nyek. Legyen sz\u00f3 hagyom\u00e1nyos k\u00ednai gy\u00f3gy\u00e1szati f\u0151zetdarabokr\u00f3l, t\u00f6rt fal\u00fa f\u0151zetdarabokr\u00f3l, hagyom\u00e1nyos k\u00ednai gy\u00f3gy\u00e1szati formula granul\u00e1tumr\u00f3l \u00e9s egy\u00e9b \u00faj k\u00ednai gy\u00f3gy\u00e1szati f\u0151zetdarabokr\u00f3l, ezeket mind f\u0151zet vagy v\u00edzzel val\u00f3 \u00e1t\u00f6bl\u00edt\u00e9s \u00fatj\u00e1n szedik. Ez\u00e9rt nagy jelent\u0151s\u00e9ge van annak, hogy a standard dekokci\u00f3s kutat\u00e1st prefer\u00e1lt kontrollk\u00e9nt haszn\u00e1lj\u00e1k m\u00e1s k\u00ednai gy\u00f3gyszerk\u00e9sz\u00edtm\u00e9nyek vizsg\u00e1lat\u00e1hoz. Ez a tanulm\u00e1ny megvil\u00e1g\u00edtja a mennyis\u00e9gi \u00e1tviteli t\u00f6rv\u00e9nyt a f\u0151zetdarabokr\u00f3l a standard f\u0151zetekre, megalapozva ezzel a verbena hagyom\u00e1nyos k\u00ednai gy\u00f3gyszerk\u00e9sz\u00edtm\u00e9nyek kutat\u00e1s\u00e1t \u00e9s min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9s\u00e9t.
\nEz a tanulm\u00e1ny a verbaszkozid, az 5-hidroxi-verbaszkozid \u00e9s a verbaszkozid verbaszkozid szeletekben t\u00f6rt\u00e9n\u0151 el\u0151\u00e1ll\u00edt\u00e1s\u00e1ra \u00f6sszpontos\u00edt, \u00e9s meg\u00e1llap\u00edtja az UPLC jellegzetes t\u00e9rk\u00e9p\u00e9t. A t\u00e9rk\u00e9pinform\u00e1ci\u00f3t k\u00e9miai m\u00f3delemz\u00e9ssel elemezz\u00fck, \u00e9s a verbaszkozid, az 5-hidroxi-verbaszkozid \u00e9s a verbaszkozid verbaszkozidban l\u00e9v\u0151 verbaszkozid tartalm\u00e1t egyszerre hat\u00e1rozzuk meg ultra-nagy teljes\u00edtm\u00e9ny\u0171 folyad\u00e9kkromatogr\u00e1fi\u00e1val, kombin\u00e1lva egy teszt t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si m\u00f3dszerrel. Az eredm\u00e9nyeket \u00f6sszehasonl\u00edtjuk a k\u00fcls\u0151 standard m\u00f3dszerrel kapott eredm\u00e9nyekkel. \u00c9s m\u00e9rje meg a standard f\u0151zet hozam\u00e1t, a verbaszkozid, az 5-hidroxi-verbaszkozid \u00e9s a verbaszkozid tartalm\u00e1t, sz\u00e1m\u00edtsa ki az \u00e1tviteli ar\u00e1nyt, \u00e9s ez alapj\u00e1n v\u00e9gezzen tanulm\u00e1nyt a verbaszkozid f\u0151zetdarabok \u00e1tvitel\u00e9r\u0151l a standard f\u0151zetbe a k\u00fcl\u00f6nb\u00f6z\u0151 min\u0151s\u00e9gi mutat\u00f3k racionalit\u00e1s\u00e1nak bizony\u00edt\u00e1s\u00e1ra.<\/p>\n

\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"\"
\nA verb\u00e9na minta jellegzetes spektrum\u00e1nak izokratikus el\u00faci\u00f3j\u00e1val nem lehet el\u00e9rni az alapvonali elv\u00e1laszt\u00e1st, ez\u00e9rt gradiens el\u00faci\u00f3t alkalmaztunk. Az el\u0151zetes k\u00eds\u00e9rletek sor\u00e1n ebben a tanulm\u00e1nyban olyan mobilf\u00e1zisokat hasonl\u00edtottunk \u00f6ssze, mint a metanol-v\u00edz, acetonitril-v\u00edz, acetonitril-0,1% foszforsavoldat \u00e9s acetonitril-0,05% foszforsavoldat. V\u00e9g\u00fcl az acetonitril-0,05% foszforsavoldatot v\u00e1lasztott\u00e1k mobil f\u00e1zisnak. A fenti kromatogr\u00e1fi\u00e1s k\u00f6r\u00fclm\u00e9nyek k\u00f6z\u00f6tt a kromatogr\u00e1fi\u00e1s cs\u00facsok elv\u00e1laszt\u00e1sa, az elm\u00e9leti lemezsz\u00e1m \u00e9s a cs\u00facs alakj\u00e1nak param\u00e9terei mind j\u00f3k voltak. Ez a tanulm\u00e1ny egyt\u00e9nyez\u0151s k\u00eds\u00e9rleti rendszert haszn\u00e1lt az extrakci\u00f3s old\u00f3szer, az extrakci\u00f3s m\u00f3dszer \u00e9s id\u0151, valamint a szil\u00e1rd-folyad\u00e9k ar\u00e1ny hat\u00e1s\u00e1nak vizsg\u00e1lat\u00e1ra az extrakci\u00f3 hat\u00e9konys\u00e1g\u00e1ra. Az eredm\u00e9nyek azt mutatt\u00e1k, hogy az extrakci\u00f3s hat\u00e9konys\u00e1g akkor volt a legmagasabb, amikor az extrakci\u00f3s old\u00f3szer 80% metanol volt, a szil\u00e1rd-folyad\u00e9k ar\u00e1ny 1:50 (g\/ml) volt, \u00e9s a reflux extrakci\u00f3t 120 percig v\u00e9gezt\u00fck. Ez\u00e9rt a fenti m\u00f3dszert haszn\u00e1ltuk a verb\u00e9na szeletek extrakci\u00f3s m\u00f3dszerek\u00e9nt.
\nA hagyom\u00e1nyos k\u00ednai orvosl\u00e1sban a t\u00f6bb index\u0171 \u00f6sszetev\u0151k \u00e1tfog\u00f3 min\u0151s\u00e9gellen\u0151rz\u00e9se elker\u00fclhetetlen tendenci\u00e1v\u00e1 v\u00e1lt a hagyom\u00e1nyos k\u00ednai orvosl\u00e1s min\u0151s\u00e9gellen\u0151rz\u00e9s\u00e9nek fejl\u0151d\u00e9s\u00e9ben. A jellemz\u0151\/ujjlenyomat-spektrum hat\u00e9kony min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9si m\u00f3dszer, \u00e9s az egy teszt t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si elemz\u00e9si m\u00f3dszerrel kombin\u00e1lva el\u00e9rheti a min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9s integrit\u00e1s\u00e1t \u00e9s pontoss\u00e1g\u00e1t. Ez a tanulm\u00e1ny l\u00e9trehozta a verbaszkozid f\u0151zetdarabok UPLC karakterisztikus t\u00e9rk\u00e9p\u00e9t, azonos\u00edtott 5 k\u00f6z\u00f6s cs\u00facsot \u00e9s azonos\u00edtott 3 komponenst. Az elemz\u00e9si id\u0151 jelent\u0151sen ler\u00f6vid\u00fclt a HPLC-hez k\u00e9pest, \u00e9s a kromatogr\u00e1fi\u00e1s felt\u00e9telek felhaszn\u00e1lhat\u00f3k az 5-hidroxi-verbaszkozid, a verbaszkozid \u00e9s a verbaszkozid-tartalom meghat\u00e1roz\u00e1s\u00e1ra. A f\u0151komponens-elemz\u00e9st a jellemz\u0151 cs\u00facsok cs\u00facster\u00fclet\u00e9n v\u00e9gezt\u00fck el, \u00e9s a f\u0151komponensek \u00e1tfog\u00f3 \u00e9rt\u00e9kel\u00e9si modellje tov\u00e1bb jav\u00edtotta a verb\u00e9na min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9si \u00e9s elemz\u00e9si m\u00f3dszer\u00e9t.<\/p>\n

A 2020-as K\u00ednai Gy\u00f3gyszerk\u00f6nyvben a verb\u00e9na tartalom meghat\u00e1roz\u00e1si indexe az oleanolsav \u00e9s az ursolsav teljes mennyis\u00e9ge, amelyek mindketten alacsony polarit\u00e1s\u00fa \u00e9s alacsony v\u00edzold\u00e9konys\u00e1g\u00fa triterpenoidok. Az el\u0151zetes k\u00eds\u00e9rleti kutat\u00e1si eredm\u00e9nyek azt mutatj\u00e1k, hogy a verbena standard f\u0151zet\u00e9ben az oleanolsav \u00e9s az ursolsav \u00f6sszes tartalma kevesebb, mint 2,0 mg\/g, \u00e9s az \u00e1tad\u00e1si ar\u00e1ny kevesebb, mint 6%. Ez\u00e9rt a tulajdons\u00e1gt\u00e9rk\u00e9p alapj\u00e1n egy t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si m\u00f3dszert hoztak l\u00e9tre az 5-hidroxi-verbaszkozid, a verbaszkozid \u00e9s a verbaszkozid tartalm\u00e1nak meghat\u00e1roz\u00e1s\u00e1ra. A verb\u00e9na pol\u00e1ris komponensei f\u0151k\u00e9nt ciklohex\u00e9n\u00e9terterp\u00e9nek, amelyek k\u00f6z\u00fcl a verbaszkozid \u00e9s az 5-hidroxi-verbaszkozid a legnagyobb tartalm\u00fa f\u0151 komponensek, \u00e9s a standard f\u0151zetnek magasabb az \u00e1tad\u00e1si ar\u00e1nya. Egyes t\u00e9telek \u00e1tad\u00e1si sebess\u00e9ge meghaladja az 100%-t, m\u00edg az 5-hidroxi-verbaszkozid \u00e9s a verbaszkozid teljes \u00e1tad\u00e1si tartom\u00e1nya 56,6% \u00e9s 91,2% k\u00f6z\u00f6tt van. Ennek lehets\u00e9ges oka, hogy a hasonl\u00f3 komponensek szerkezeti \u00e1talakul\u00e1son mennek kereszt\u00fcl a meleg\u00edt\u00e9s, forral\u00e1s \u00e9s egy\u00e9b folyamatok sor\u00e1n. A verbaszkozid, az 5-hidroxi-verbaszkozid \u00e9s a verbaszkozid tartalm\u00e1ban \u00e9s \u00e1tad\u00e1si sebess\u00e9g\u00e9ben k\u00fcl\u00f6nbs\u00e9gek vannak a verbaszkozid standard f\u0151zet\u00e9nek 18 t\u00e9tele k\u00f6z\u00f6tt, ami \u00f6sszef\u00fcgghet a f\u0151zetdarabok tartalm\u00e1val \u00e9s text\u00far\u00e1j\u00e1val. Egyes f\u0151zetdarabok vil\u00e1gosabb sz\u00edn\u0171ek, hosszabb a t\u00e1rol\u00e1si idej\u00fck, \u00e9s t\u00f6bb a feldolgoz\u00e1s sor\u00e1n keletkezett t\u00f6rmel\u00e9k, ami a tartalom \u00e9s az \u00e1tad\u00e1si ar\u00e1ny nagym\u00e9rt\u00e9k\u0171 ingadoz\u00e1s\u00e1nak oka lehet. A h\u00e1rom kiv\u00e1lasztott \u00f6sszetev\u0151nek magas a verbena tartalma, \u00e9s j\u00f3 farmakol\u00f3giai aktivit\u00e1ssal rendelkeznek antioxid\u00e1ns, m\u00e1jv\u00e9d\u0151, neuroprotekt\u00edv, sz\u00edv- \u00e9s agyi iszk\u00e9mia elleni v\u00e9d\u0151, gyullad\u00e1scs\u00f6kkent\u0151 \u00e9s egy\u00e9b szempontb\u00f3l. Ezek a verbena egyik f\u0151 anyagi alapj\u00e1t k\u00e9pezik farmakol\u00f3giai hat\u00e1sainak kifejt\u00e9s\u00e9hez.<\/p>\n

Az egy tesztb\u0151l \u00e1ll\u00f3, t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si m\u00f3dszer eredm\u00e9nyei nem mutattak szignifik\u00e1ns k\u00fcl\u00f6nbs\u00e9get a k\u00fcls\u0151 standard m\u00f3dszerhez k\u00e9pest, \u00e9s felhaszn\u00e1lhat\u00f3 a verb\u00e9na t\u00f6bb \u00f6sszetev\u0151j\u00e9nek mennyis\u00e9gi elemz\u00e9s\u00e9re. Az UPLC funkci\u00f3t\u00e9rk\u00e9p kombin\u00e1lva a t\u00f6bb indexkomponens\u0171 egy m\u00e9r\u00e9ses t\u00f6bbsz\u00f6r\u00f6s \u00e9rt\u00e9kel\u00e9si m\u00f3dszerrel hivatkoz\u00e1si alapot ny\u00fajthat a verb\u00e9na \u00e9s a verb\u00e9na k\u00ednai gy\u00f3gyn\u00f6v\u00e9nyk\u00e9sz\u00edtm\u00e9nyek gy\u00e1rt\u00e1si folyamat\u00e1nak kutat\u00e1s\u00e1hoz \u00e9s min\u0151s\u00e9g\u00e9rt\u00e9kel\u00e9s\u00e9hez.<\/p>","protected":false},"excerpt":{"rendered":"

Research on the Quality Evaluation of Verbena and the Transfer Law of Standard Decoction Dosage Based on UPLC Feature Map and One Test Multiple Evaluation Method Verbena officinalis L., a dry aboveground part of the Verbena officinalis L. plant in the Verbenaceae family, was first recorded in the “Catalogue of Famous Physicians” and classified as […]<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[20],"tags":[],"yoast_head":"\nResearch on the Quality Evaluation of Verbena and the Transfer Law of Standard Decoction Dosage Based on UPLC Feature Map and One Test Multiple Evaluation Method - China Chemical Manufacturer<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/longchangextracts.com\/hu\/verbena\/\" \/>\n<meta property=\"og:locale\" content=\"hu_HU\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Research on the Quality Evaluation of Verbena and the Transfer Law of Standard Decoction Dosage Based on UPLC Feature Map and One Test Multiple Evaluation Method - 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