{"id":4077,"date":"2024-08-04T08:21:45","date_gmt":"2024-08-04T08:21:45","guid":{"rendered":"https:\/\/longchangextracts.com\/?p=4077"},"modified":"2024-08-04T08:21:45","modified_gmt":"2024-08-04T08:21:45","slug":"anion-resins","status":"publish","type":"post","link":"https:\/\/longchangextracts.com\/hu\/anion-resins\/","title":{"rendered":"Tanulm\u00e1ny az oleuropein anionos gyant\u00e1val t\u00f6rt\u00e9n\u0151 elv\u00e1laszt\u00e1s\u00e1nak folyamat\u00e1r\u00f3l \u00e9s teljes\u00edtm\u00e9ny\u00e9r\u0151l"},"content":{"rendered":"<p>Tanulm\u00e1ny az oleuropein anionos gyant\u00e1val t\u00f6rt\u00e9n\u0151 elv\u00e1laszt\u00e1s\u00e1nak folyamat\u00e1r\u00f3l \u00e9s teljes\u00edtm\u00e9ny\u00e9r\u0151l<br \/>\nAz Olea europaea L. az olajfaf\u00e9l\u00e9k (Oleaceae) csal\u00e1dj\u00e1ba \u00e9s az olajfaf\u00e9l\u00e9k (Oleaceae) nemzets\u00e9g\u00e9be tartoz\u00f3 \u00f6r\u00f6kz\u00f6ld fa. K\u00edn\u00e1ban \u00e9s a mediterr\u00e1n orsz\u00e1gokban sz\u00e9les k\u00f6rben \u00fcltetik, \u00e9s ezekben az orsz\u00e1gokban \u00e9s r\u00e9gi\u00f3kban az egyik legfontosabb mez\u0151gazdas\u00e1gi haszonn\u00f6v\u00e9ny. Jelenleg az olajbogy\u00f3-forr\u00e1sok fejleszt\u00e9se \u00e9s hasznos\u00edt\u00e1sa els\u0151sorban a gy\u00fcm\u00f6lcs\u00f6k hasznos\u00edt\u00e1s\u00e1ra \u00f6sszpontos\u00edt, m\u00edg az olajfaleveleket hullad\u00e9kk\u00e9nt hagyj\u00e1k el az \u00fcltetv\u00e9nyekben, ami nagy er\u0151forr\u00e1s-pazarl\u00e1st okoz. A modern kutat\u00e1sok meg\u00e1llap\u00edtott\u00e1k, hogy az olajfalev\u00e9l b\u0151s\u00e9gesen tartalmaz iridoid glikozidokat, fenolokat, pentaciklusos triterpenoidokat \u00e9s flavonoidokat. Ezek k\u00f6z\u00fcl az oleuropein (OL) a legakt\u00edvabb anyag, amely antioxid\u00e1ns, v\u00edrusellenes, bakt\u00e9rium\u00f6l\u0151 \u00e9s gyullad\u00e1scs\u00f6kkent\u0151, hipoglik\u00e9mi\u00e1s, v\u00e9rnyom\u00e1scs\u00f6kkent\u0151, r\u00e1kellenes \u00e9s egy\u00e9b hat\u00e1sokkal rendelkezik, \u00e9s sz\u00e9les k\u00f6rben haszn\u00e1lj\u00e1k az \u00e9lelmiszeriparban, a gy\u00f3gy\u00e1szatban, a kozmetikumokban \u00e9s m\u00e1s ter\u00fcleteken. Az OL az iridoid glikozidok oszt\u00e1ly\u00e1ba tartozik, amelyek k\u00f6nnyen old\u00f3dnak old\u00f3szerekben, p\u00e9ld\u00e1ul v\u00edzben, etanolban \u00e9s metanolban. Olyan k\u00f6r\u00fclm\u00e9nyek k\u00f6z\u00f6tt, mint sav, l\u00fag, magas h\u0151m\u00e9rs\u00e9klet \u00e9s f\u00e9ny, k\u00f6nnyen bomlanak hidroxitirozoll\u00e1.<br \/>\nJelenleg az OL elv\u00e1laszt\u00e1s\u00e1nak f\u0151 m\u00f3dszerei k\u00f6z\u00e9 tartozik a makropor\u00f3zus gyantaadszorpci\u00f3, a nagy sebess\u00e9g\u0171 ellen\u00e1ram\u00fa extrakci\u00f3 \u00e9s a szuperkritikus extrakci\u00f3. Ezek k\u00f6z\u00fcl a nagysebess\u00e9g\u0171 ellen\u00e1ram\u00fa extrakci\u00f3 \u00e9s a szuperkritikus extrakci\u00f3 jobb elv\u00e1laszt\u00e1si hat\u00e1ssal rendelkezik, \u00e9s nagy tisztas\u00e1g\u00fa OL-t nyerhet\u00fcnk. Ez a k\u00e9t m\u00f3dszer azonban nagy mennyis\u00e9g\u0171 berendez\u00e9st \u00e9s szem\u00e9lyzetet ig\u00e9nyel, \u00e9s nem alkalmas nagy\u00fczemi ipari termel\u00e9sre. A makrop\u00f3rusos gyanta por\u00f3zus szerkezettel \u00e9s kiv\u00e1l\u00f3 adszorpci\u00f3s teljes\u00edtm\u00e9nnyel rendelkezik, \u00e9s sz\u00e9les k\u00f6rben haszn\u00e1lj\u00e1k a n\u00f6v\u00e9nyi hat\u00f3anyagok d\u00fas\u00edt\u00e1s\u00e1ra, elv\u00e1laszt\u00e1s\u00e1ra \u00e9s tiszt\u00edt\u00e1s\u00e1ra. Az OL makrop\u00f3rusos gyant\u00e1val t\u00f6rt\u00e9n\u0151 d\u00fas\u00edt\u00e1s\u00e1nak \u00e9s elv\u00e1laszt\u00e1s\u00e1nak f\u0151 mechanizmusa az, hogy a k\u00e9t hat\u00f3anyag bizonyos k\u00f6r\u00fclm\u00e9nyek k\u00f6z\u00f6tt hidrog\u00e9nk\u00f6t\u00e9sen \u00e9s van der Waals-er\u0151k\u00f6n kereszt\u00fcl reverzibilis k\u00f6lcs\u00f6nhat\u00e1sba l\u00e9phet, ez\u00e1ltal szelekt\u00edven d\u00fas\u00edtja \u00e9s elv\u00e1lasztja \u0151ket az extrakci\u00f3s oldatb\u00f3l. Az elm\u00falt \u00e9vekben sz\u00e1mos tud\u00f3s foglalkozott az OL d\u00fas\u00edt\u00e1s\u00e1val \u00e9s elv\u00e1laszt\u00e1s\u00e1val olajfalev\u00e9l-kivonatokban, nem pol\u00e1ros \u00e9s gyeng\u00e9n pol\u00e1ros gyant\u00e1k felhaszn\u00e1l\u00e1s\u00e1val. Tian \u00e9s munkat\u00e1rsai a D101 makropor\u00f3zus gyant\u00e1t haszn\u00e1lt\u00e1k az OL d\u00fas\u00edt\u00e1s\u00e1ra \u00e9s elv\u00e1laszt\u00e1s\u00e1ra, \u00e9s etil-acet\u00e1t extrakci\u00f3val 63,43% tisztas\u00e1g\u00fa OL term\u00e9ket nyertek. Wang \u00e9s munkat\u00e1rsai AB-8 gyant\u00e1t haszn\u00e1ltak az OL d\u00fas\u00edt\u00e1s\u00e1ra \u00e9s elv\u00e1laszt\u00e1s\u00e1ra, \u00e9s a tisztas\u00e1g 9,16%-r\u0151l 20,38%-re n\u0151tt. Sahin \u00e9s munkat\u00e1rsai meg\u00e1llap\u00edtott\u00e1k, hogy a XAD 7HP gyanta OL-adszorpci\u00f3j\u00e1nak mechanizmusa kv\u00e1zi m\u00e1sodrend\u0171 kinetik\u00e1nak felel meg. Liu \u00e9s munkat\u00e1rsai meg\u00e1llap\u00edtott\u00e1k, hogy a BMKX-4 makropor\u00f3zus adszorpci\u00f3s gyanta \u00e1ltal t\u00f6rt\u00e9n\u0151 OL-d\u00fas\u00edt\u00e1s mechanizmusa megfelel a kv\u00e1zi m\u00e1sodrend\u0171 kinetik\u00e1nak \u00e9s a Freundlich-modellnek, \u00e9s 47,59%-re n\u00f6veli az OL tisztas\u00e1g\u00e1t. Elm\u00e9letileg az OL a polifenolos vegy\u00fcletek k\u00f6z\u00e9 tartozik, \u00e9s az anionos gyanta adszorpci\u00f3s mechanizmusa k\u00e9pes el\u00e9rni a d\u00fas\u00edt\u00e1st \u00e9s az elv\u00e1laszt\u00e1st. Az OL aniongyant\u00e1s elv\u00e1laszt\u00e1s\u00e1nak kutat\u00e1s\u00e1r\u00f3l azonban m\u00e9g nem k\u00e9sz\u00fcltek jelent\u00e9sek. Ez\u00e9rt aniongyant\u00e1t (LX-68M) haszn\u00e1ltunk az OL statikus \u00e9s dinamikus adszorpci\u00f3s \u00e9s deszorpci\u00f3s tulajdons\u00e1gainak tanulm\u00e1nyoz\u00e1s\u00e1ra, \u00e9s tov\u00e1bb vizsg\u00e1ltuk az OL sziv\u00e1rg\u00e1si g\u00f6rb\u00e9j\u00e9t, el\u00faci\u00f3s g\u00f6rb\u00e9j\u00e9t \u00e9s az OL aniongyanta regener\u00e1ci\u00f3j\u00e1nak stabilit\u00e1s\u00e1t, hogy elm\u00e9leti referenci\u00e1t ny\u00fajtsunk az OL \u00e9s hasonl\u00f3 term\u00e9szetes term\u00e9kek aniongyant\u00e1val t\u00f6rt\u00e9n\u0151 d\u00fas\u00edt\u00e1s\u00e1hoz, elv\u00e1laszt\u00e1s\u00e1hoz, tiszt\u00edt\u00e1s\u00e1hoz.<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4078\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/1-31.png\" alt=\"\" width=\"1044\" height=\"394\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/1-31.png 1044w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/1-31-768x290.png 768w\" sizes=\"(max-width: 1044px) 100vw, 1044px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4079\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/2-29.png\" alt=\"\" width=\"691\" height=\"301\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4080\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/3-28.png\" alt=\"\" width=\"1044\" height=\"388\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/3-28.png 1044w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/3-28-768x285.png 768w\" sizes=\"(max-width: 1044px) 100vw, 1044px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4081\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/4-26.png\" alt=\"\" width=\"1064\" height=\"454\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/4-26.png 1064w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/4-26-768x328.png 768w\" sizes=\"(max-width: 1064px) 100vw, 1064px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4082\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/5-24.png\" alt=\"\" width=\"1082\" height=\"384\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/5-24.png 1082w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/5-24-768x273.png 768w\" sizes=\"(max-width: 1082px) 100vw, 1082px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4083\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/6-24.png\" alt=\"\" width=\"1096\" height=\"348\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/6-24.png 1096w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/6-24-768x244.png 768w\" sizes=\"(max-width: 1096px) 100vw, 1096px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4084\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/7-22.png\" alt=\"\" width=\"1084\" height=\"372\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/7-22.png 1084w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/7-22-768x264.png 768w\" sizes=\"(max-width: 1084px) 100vw, 1084px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4085\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/8-17.png\" alt=\"\" width=\"1086\" height=\"212\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/8-17.png 1086w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/8-17-768x150.png 768w\" sizes=\"(max-width: 1086px) 100vw, 1086px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4086\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/9-14.png\" alt=\"\" width=\"1050\" height=\"452\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/9-14.png 1050w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/9-14-768x331.png 768w\" sizes=\"(max-width: 1050px) 100vw, 1050px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4087\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/10-10.png\" alt=\"\" width=\"1060\" height=\"312\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/10-10.png 1060w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/10-10-768x226.png 768w\" sizes=\"(max-width: 1060px) 100vw, 1060px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4088\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/11-9.png\" alt=\"\" width=\"1092\" height=\"312\" srcset=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/11-9.png 1092w, https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/11-9-768x219.png 768w\" sizes=\"(max-width: 1092px) 100vw, 1092px\" \/><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-full wp-image-4089\" src=\"https:\/\/longchangextracts.com\/wp-content\/uploads\/2024\/08\/12-8.png\" alt=\"\" width=\"757\" height=\"312\" \/><\/p>\n<p>Az izotermikus adszorpci\u00f3s k\u00eds\u00e9rlet eredm\u00e9nyei azt mutatj\u00e1k, hogy a Freundlich-f\u00e9le izotermikus adszorpci\u00f3s modell j\u00f3l le\u00edrja az LX-68M gyanta OL adszorpci\u00f3s folyamat\u00e1t a k\u00eds\u00e9rleti h\u0151m\u00e9rs\u00e9kleten, R2=0,9642 korrel\u00e1ci\u00f3s egy\u00fctthat\u00f3val, ami azt jelzi, hogy az adszorpci\u00f3 kedvez\u0151. Az OL LX-68M gyanta \u00e1ltali adszorpci\u00f3ja ink\u00e1bb az \u00e1l-m\u00e1sodrend\u0171 kinetik\u00e1nak felel meg, R2=0,9934 \u00e9rt\u00e9kkel, ami azt jelzi, hogy az OL LX-68M gyanta \u00e1ltali adszorpci\u00f3ja egyszerre t\u00f6rt\u00e9nik fizikai adszorpci\u00f3 \u00e9s k\u00e9miai adszorpci\u00f3 r\u00e9v\u00e9n, a k\u00e9miai adszorpci\u00f3 a f\u0151 mechanizmus. A mechanizmus a gyanta \u00e9s az OL funkci\u00f3s csoportjai k\u00f6z\u00f6tti k\u00e9miai k\u00f6t\u00e9sek kialakul\u00e1sa lehet. A statikus \u00e9s dinamikus adszorpci\u00f3s \u00e9s deszorpci\u00f3s k\u00eds\u00e9rletekkel kapott optim\u00e1lis elv\u00e1laszt\u00e1si felt\u00e9telek a k\u00f6vetkez\u0151k: 0,25 g\/ml extrakci\u00f3s koncentr\u00e1ci\u00f3, 45% etanol eluens, 2,0BV\/h t\u00f6lt\u00e9si sebess\u00e9g, 6 t\u00f6lt\u00e9si t\u00e9rfogat.0BV, a deszorpci\u00f3s sebess\u00e9g 2,0BV\/h, \u00e9s a deszorpci\u00f3s t\u00e9rfogat 10,0BV; Ekkor az adszorpci\u00f3s sebess\u00e9g \u00e9s a deszorpci\u00f3s sebess\u00e9g 86,86% \u00e9s 87,08% volt, \u00e9s a kapott OL tisztas\u00e1ga 52,33% volt. A gyantaadszorpci\u00f3s deszorpci\u00f3 4 ciklusa ut\u00e1n az adszorpci\u00f3s hat\u00e9konys\u00e1g 54,9% volt. A regener\u00e1l\u00e1s ut\u00e1n az adszorpci\u00f3s r\u00e1ta el\u00e9rte a kezdeti adszorpci\u00f3s r\u00e1ta 93,1%-j\u00e9t, ami azt jelzi, hogy a gyanta a regener\u00e1l\u00e1s ut\u00e1n is j\u00f3 adszorpci\u00f3s teljes\u00edtm\u00e9nyt ny\u00fajt. A fenti eredm\u00e9nyek azt mutatj\u00e1k, hogy az LX-68M gyanta j\u00f3 d\u00fas\u00edt\u00e1si, elv\u00e1laszt\u00e1si \u00e9s tiszt\u00edt\u00e1si hat\u00e9konys\u00e1ggal rendelkezik az OL eset\u00e9ben, \u00e9s a megl\u00e9v\u0151 elj\u00e1r\u00e1sokkal \u00f6sszehasonl\u00edtva ez az elj\u00e1r\u00e1s szobah\u0151m\u00e9rs\u00e9kleten \u00e9s nyom\u00e1son m\u0171k\u00f6dik, biztons\u00e1gos \u00e9s egyszer\u0171, valamint z\u00f6ld \u00e9s nem m\u00e9rgez\u0151 old\u00f3szereket haszn\u00e1l. Elm\u00e9leti kutat\u00e1si alapot \u00e9s technikai t\u00e1mogat\u00e1st ny\u00fajthat az anionos gyanta alkalmaz\u00e1s\u00e1hoz az OL \u00e9s hasonl\u00f3 term\u00e9szetes term\u00e9kek ipari elv\u00e1laszt\u00e1s\u00e1ban \u00e9s tiszt\u00edt\u00e1s\u00e1ban. B\u00e1r ez a tanulm\u00e1ny az LX-68M gyanta adszorpci\u00f3s folyamat\u00e1t vizsg\u00e1lta az OL-on, a szennyez\u0151d\u00e9sek \u00e9s az OL k\u00f6z\u00f6tti kompetit\u00edv adszorpci\u00f3s viselked\u00e9snek is lehet bizonyos hat\u00e1sa az elv\u00e1laszt\u00e1s hat\u00e9konys\u00e1g\u00e1ra. Ez\u00e9rt tov\u00e1bbi kutat\u00e1sokra van sz\u00fcks\u00e9g a megfelel\u0151 adszorpci\u00f3s mechanizmus meghat\u00e1roz\u00e1s\u00e1hoz, \u00e9s elm\u00e9leti alapot kell biztos\u00edtani az LX-68M gyanta tov\u00e1bbi fejleszt\u00e9s\u00e9hez \u00e9s felhaszn\u00e1l\u00e1s\u00e1hoz.<\/p>","protected":false},"excerpt":{"rendered":"<p>Study on the Process and Performance of Separation of Oleuropein by Anionic Resin Olea europaea L. is an evergreen tree belonging to the Oleaceae family and the Oleaceae genus. It is widely planted in China and Mediterranean countries and is one of the main agricultural cash crops in these countries and regions. At present, the [&hellip;]<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[20],"tags":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v23.0 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Study on the Process and Performance of Separation of Oleuropein by Anionic Resin - China Chemical Manufacturer<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/longchangextracts.com\/hu\/anion-resins\/\" \/>\n<meta property=\"og:locale\" content=\"hu_HU\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"Study on the Process and Performance of Separation of Oleuropein by Anionic Resin - China Chemical Manufacturer\" \/>\n<meta property=\"og:description\" content=\"Study on the Process and Performance of Separation of Oleuropein by Anionic Resin Olea europaea L. is an evergreen tree belonging to the Oleaceae family and the Oleaceae genus. It is widely planted in China and Mediterranean countries and is one of the main agricultural cash crops in these countries and regions. 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